Jan K. Cermak, Karel Kolar and Vladimir Cirkva Pages 126 - 130 ( 5 )
The microwave-assisted synthesis of N-alkylbenzamides from benzoic acid and primary aliphatic amines has been developed under solvent-free conditions. The different solid catalysts have been investigated. The suggested synthesis is environmentally friendly and excellent yields (97 - 99 %) have been reached.
Amino-de-hydroxylation, heterogenous catalyst, microporous materials, microwave assisted synthesis, Nalkylbenzamides, solvent-free reaction
Environmental Process Engineering Laboratory, Institute of Chemical Process Fundamentals of the ASCR, Rozvojova 135, 165 02 Prague, Czech Republic.